The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction

K. L Samuel Lai, C. Y. Tan, S. Ramesh, R. Tolouei, Boon Kar Yap, M. Amiriyan

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

The effect of ball milling hours on the manufacture of nano-crystalline forsterite powder was investigated in terms of particle size and phase stability. A quasi-mechanical activation method followed by heat treatment was successfully employed to produce nano-crystalline forsterite powder. During the attempt, ball milling hours were manipulated to study its effects on the particle size. XRD analysis was then conducted on the heat treated powders to determine the critical particle size. Based on XRD traces, it was revealed that 7 hours of low-energy ball milling was sufficient to produce crystalline forsterite powders. Subsequent FWHM studies also affirmed the critical particle size (≈ 41 nm) required to successfully transform MgO and Mg 3Si4O10(OH)2 into pure forsterite powder.

Original languageEnglish
Title of host publication5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011
Pages102-104
Number of pages3
Volume35 IFMBE
DOIs
Publication statusPublished - 2011
Event5th Kuala Lumpur International Conference on Biomedical Engineering, BIOMED 2011, Held in Conjunction with the 8th Asian Pacific Conference on Medical and Biological Engineering, APCMBE 2011 - Kuala Lumpur, Malaysia
Duration: 20 Jun 201123 Jun 2011

Other

Other5th Kuala Lumpur International Conference on Biomedical Engineering, BIOMED 2011, Held in Conjunction with the 8th Asian Pacific Conference on Medical and Biological Engineering, APCMBE 2011
CountryMalaysia
CityKuala Lumpur
Period20/06/1123/06/11

Fingerprint

Ball milling
Solid state reactions
Particle size
Powders
Crystalline materials
Nanocrystalline powders
Phase stability
Full width at half maximum
Chemical activation
Heat treatment
forsterite

All Science Journal Classification (ASJC) codes

  • Biomedical Engineering
  • Bioengineering

Cite this

Lai, K. L. S., Tan, C. Y., Ramesh, S., Tolouei, R., Yap, B. K., & Amiriyan, M. (2011). The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction. In 5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011 (Vol. 35 IFMBE, pp. 102-104) https://doi.org/10.1007/978-3-642-21729-6_28
Lai, K. L Samuel ; Tan, C. Y. ; Ramesh, S. ; Tolouei, R. ; Yap, Boon Kar ; Amiriyan, M. / The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction. 5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011. Vol. 35 IFMBE 2011. pp. 102-104
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abstract = "The effect of ball milling hours on the manufacture of nano-crystalline forsterite powder was investigated in terms of particle size and phase stability. A quasi-mechanical activation method followed by heat treatment was successfully employed to produce nano-crystalline forsterite powder. During the attempt, ball milling hours were manipulated to study its effects on the particle size. XRD analysis was then conducted on the heat treated powders to determine the critical particle size. Based on XRD traces, it was revealed that 7 hours of low-energy ball milling was sufficient to produce crystalline forsterite powders. Subsequent FWHM studies also affirmed the critical particle size (≈ 41 nm) required to successfully transform MgO and Mg 3Si4O10(OH)2 into pure forsterite powder.",
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Lai, KLS, Tan, CY, Ramesh, S, Tolouei, R, Yap, BK & Amiriyan, M 2011, The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction. in 5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011. vol. 35 IFMBE, pp. 102-104, 5th Kuala Lumpur International Conference on Biomedical Engineering, BIOMED 2011, Held in Conjunction with the 8th Asian Pacific Conference on Medical and Biological Engineering, APCMBE 2011, Kuala Lumpur, Malaysia, 20/06/11. https://doi.org/10.1007/978-3-642-21729-6_28

The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction. / Lai, K. L Samuel; Tan, C. Y.; Ramesh, S.; Tolouei, R.; Yap, Boon Kar; Amiriyan, M.

5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011. Vol. 35 IFMBE 2011. p. 102-104.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

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Lai KLS, Tan CY, Ramesh S, Tolouei R, Yap BK, Amiriyan M. The effect of ball milling hours in the synthesizing nano-crystalline forsterite via solid-state reaction. In 5th Kuala Lumpur International Conference on Biomedical Engineering 2011, BIOMED 2011. Vol. 35 IFMBE. 2011. p. 102-104 https://doi.org/10.1007/978-3-642-21729-6_28