Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide

S. H. Sarijo, M. L. Jadam, Zaemah Jubri @ Mohd Zufri

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

A nonsteroidal drug, flufenamic acid (FA) was successfully intercalated into magnesiumaluminium-layered double hydroxide, MAL for the formation of magnesium-aluminiumflufenamate-layered double hydroxide, MAF by self-assembly technique. As a result of the successful intercalation, basal spacing increased from 9.8 Å in the MAL to 23.5 Å in the MAF hybrid nanocomposite. The FTIR spectra of the MAF hybrid nanocomposite show resemblance peaks of the MAL and FA suggesting the inclusion of the organic compound into the MAL interlamellae. The percentage loading of FA was found to be 74.4 % (w/w) calculated from the percentage of carbon in the resulting material, MAF.

Original languageEnglish
Title of host publicationManufacturing Engineering and Process V
EditorsOsman Adiguzel, Mario S. Ming Kong, Kai Li
PublisherTrans Tech Publications Ltd
Pages100-103
Number of pages4
ISBN (Print)9783038357780
DOIs
Publication statusPublished - 01 Jan 2017
Event5th International Conference on Manufacturing Engineering and Process, ICMEP 2016 - Istanbul, Turkey
Duration: 25 May 201627 May 2016

Publication series

NameMaterials Science Forum
Volume887 MSF
ISSN (Print)0255-5476

Other

Other5th International Conference on Manufacturing Engineering and Process, ICMEP 2016
CountryTurkey
CityIstanbul
Period25/05/1627/05/16

Fingerprint

Flufenamic Acid
hydroxides
acids
Acids
Nanocomposites
nanocomposites
synthesis
Intercalation
organic compounds
Organic compounds
intercalation
Self assembly
Magnesium
magnesium
self assembly
drugs
Carbon
spacing
inclusions
carbon

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Sarijo, S. H., Jadam, M. L., & Jubri @ Mohd Zufri, Z. (2017). Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide. In O. Adiguzel, M. S. Ming Kong, & K. Li (Eds.), Manufacturing Engineering and Process V (pp. 100-103). (Materials Science Forum; Vol. 887 MSF). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.887.100
Sarijo, S. H. ; Jadam, M. L. ; Jubri @ Mohd Zufri, Zaemah. / Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide. Manufacturing Engineering and Process V. editor / Osman Adiguzel ; Mario S. Ming Kong ; Kai Li. Trans Tech Publications Ltd, 2017. pp. 100-103 (Materials Science Forum).
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abstract = "A nonsteroidal drug, flufenamic acid (FA) was successfully intercalated into magnesiumaluminium-layered double hydroxide, MAL for the formation of magnesium-aluminiumflufenamate-layered double hydroxide, MAF by self-assembly technique. As a result of the successful intercalation, basal spacing increased from 9.8 {\AA} in the MAL to 23.5 {\AA} in the MAF hybrid nanocomposite. The FTIR spectra of the MAF hybrid nanocomposite show resemblance peaks of the MAL and FA suggesting the inclusion of the organic compound into the MAL interlamellae. The percentage loading of FA was found to be 74.4 {\%} (w/w) calculated from the percentage of carbon in the resulting material, MAF.",
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Sarijo, SH, Jadam, ML & Jubri @ Mohd Zufri, Z 2017, Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide. in O Adiguzel, MS Ming Kong & K Li (eds), Manufacturing Engineering and Process V. Materials Science Forum, vol. 887 MSF, Trans Tech Publications Ltd, pp. 100-103, 5th International Conference on Manufacturing Engineering and Process, ICMEP 2016, Istanbul, Turkey, 25/05/16. https://doi.org/10.4028/www.scientific.net/MSF.887.100

Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide. / Sarijo, S. H.; Jadam, M. L.; Jubri @ Mohd Zufri, Zaemah.

Manufacturing Engineering and Process V. ed. / Osman Adiguzel; Mario S. Ming Kong; Kai Li. Trans Tech Publications Ltd, 2017. p. 100-103 (Materials Science Forum; Vol. 887 MSF).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

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Sarijo SH, Jadam ML, Jubri @ Mohd Zufri Z. Synthesis and physicochemical characterization of Mg-Al-flufenamate-layered double hydroxide. In Adiguzel O, Ming Kong MS, Li K, editors, Manufacturing Engineering and Process V. Trans Tech Publications Ltd. 2017. p. 100-103. (Materials Science Forum). https://doi.org/10.4028/www.scientific.net/MSF.887.100