Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite

Musdalilah Ahmad Salim, Halina Misran, Siti Zubaidah Othman, N. N.H. Shah, N. A.A. Razak, M. M. Kamisah

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Citation (Scopus)

Abstract

Monodispersed silica spheres with particles size of ca. 450 nm were successfully synthesized using modified Stöber method. The synthesized monodispersed silica spheres were successfully coated with copper through modified sol-gel method employing nonsurfactant template and catalyst. A renewable palm oil based as nonsurfactant surface modifiers, decyl-alcohol (C10) and catalyst were used to modify the silica surfaces prior to coating with copper. In order to study the effect of catalyst on copper deposition onto silica surfaces, ammonia was used as catalyst in various amounts. The X-ray diffraction patterns of Si-Cu core-shell exhibited a broad peak corresponding to amorphous silica networks and exhibited monoclinic CuO phase. It was found that samples modified in the presence of 1 ml catalyst exhibited relatively homogeneous deposition. The surface area of uncoated core (SiO2) was at ca. 7.04 m2/g and coated samples 1 ml catalyst was at ca. 8.21 m2/g.

Original languageEnglish
Title of host publicationSolid State Science and Technology IV
Pages571-574
Number of pages4
Volume895
DOIs
Publication statusPublished - 2014
Event4th International Conference on Solid State Science and Technology, ICSSST 2012 - Melaka, Malaysia
Duration: 18 Dec 201320 Dec 2013

Publication series

NameAdvanced Materials Research
Volume895
ISSN (Print)1022-6680

Other

Other4th International Conference on Solid State Science and Technology, ICSSST 2012
CountryMalaysia
CityMelaka
Period18/12/1320/12/13

Fingerprint

Surface treatment
Nanocomposites
Silica
Catalysts
Copper
Palm oil
Diffraction patterns
Sol-gel process
Ammonia
Alcohols
Particle size
X ray diffraction
Coatings

All Science Journal Classification (ASJC) codes

  • Engineering(all)

Cite this

Salim, M. A., Misran, H., Othman, S. Z., Shah, N. N. H., Razak, N. A. A., & Kamisah, M. M. (2014). Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite. In Solid State Science and Technology IV (Vol. 895, pp. 571-574). (Advanced Materials Research; Vol. 895). https://doi.org/10.4028/www.scientific.net/AMR.895.571
Salim, Musdalilah Ahmad ; Misran, Halina ; Othman, Siti Zubaidah ; Shah, N. N.H. ; Razak, N. A.A. ; Kamisah, M. M. / Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite. Solid State Science and Technology IV. Vol. 895 2014. pp. 571-574 (Advanced Materials Research).
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Salim, MA, Misran, H, Othman, SZ, Shah, NNH, Razak, NAA & Kamisah, MM 2014, Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite. in Solid State Science and Technology IV. vol. 895, Advanced Materials Research, vol. 895, pp. 571-574, 4th International Conference on Solid State Science and Technology, ICSSST 2012, Melaka, Malaysia, 18/12/13. https://doi.org/10.4028/www.scientific.net/AMR.895.571

Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite. / Salim, Musdalilah Ahmad; Misran, Halina; Othman, Siti Zubaidah; Shah, N. N.H.; Razak, N. A.A.; Kamisah, M. M.

Solid State Science and Technology IV. Vol. 895 2014. p. 571-574 (Advanced Materials Research; Vol. 895).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

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Salim MA, Misran H, Othman SZ, Shah NNH, Razak NAA, Kamisah MM. Nonsurfactant surface modifications of monodispersed Si-Cu core- shell nanocomposite. In Solid State Science and Technology IV. Vol. 895. 2014. p. 571-574. (Advanced Materials Research). https://doi.org/10.4028/www.scientific.net/AMR.895.571