Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy

Farha Mizana Shamsudin, Shahidan Radiman, Yusof Abdullah, Nasri A. Hamid

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

Oxide dispersion strengthened (ODS) ferritic alloy containing 12wt% Cr and 0.5wt% Y2O3 was prepared by mechanical alloying (MA) method and then compacted into bulk shape. Field emission scanning electron microscopy (FESEM) was performed to characterize the microstructure of milled alloy powder. The fragments and nanoclusters of Y2O3 were observed in this alloy powder. FESEM-EDS mapping on the milled alloy powder reveal the uniformity of the element distribution achieved by the alloy. The Y element is finely dispersed into the alloy matrix and the O element is observed indicating the presence of oxides throughout the alloy sample. The compacted alloy was then heat treated at 1050°C and analyzed by field emission scanning electron microscope (FESEM). The formations of nano-scale Y2O3 were observed after the heat treatment process of alloy indicating the dispersion and incorporation of Y2O3 nanoparticles into the alloy matrix.

Original languageEnglish
Title of host publication2016 UKM FST Postgraduate Colloquium
Subtitle of host publicationProceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium
EditorsKhairiah Hj. Basri, Mohd Salmi Md Noorani, Wan Zuhairi Wan Yaacob, Mohd Firdaus Mohd Yusoff, Nurul Huda Abd Karim, Mohammad Hafizuddin Hj. Jumali, Nazlina Ibrahim, Muzzneena Ahmad Mustapha, Zalita Zainuddin, Nurulkamal Masseran, Mahanem Mat Nor, Zahari Ibarahim, Noor Hayati Ahmad Rasol, Che Radziah Che Mohd Zain, Lim Seng Joe, Kamarulzaman Ibrahim, Norhayati Ahmad, Norlida Mat Daud, Syahida Che Dzul-Kifli
PublisherAmerican Institute of Physics Inc.
Volume1784
ISBN (Electronic)9780735414464
DOIs
Publication statusPublished - 17 Nov 2016
Event2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016 - Selangor, Malaysia
Duration: 13 Apr 201614 Apr 2016

Other

Other2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016
CountryMalaysia
CitySelangor
Period13/04/1614/04/16

Fingerprint

oxides
field emission
scanning electron microscopy
matrices
nanoclusters
alloying
heat treatment
electron microscopes
fragments
heat
nanoparticles
microstructure
scanning

All Science Journal Classification (ASJC) codes

  • Physics and Astronomy(all)

Cite this

Shamsudin, F. M., Radiman, S., Abdullah, Y., & A. Hamid, N. (2016). Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy. In K. H. Basri, M. S. M. Noorani, W. Z. W. Yaacob, M. F. M. Yusoff, N. H. A. Karim, M. H. H. Jumali, N. Ibrahim, M. A. Mustapha, Z. Zainuddin, N. Masseran, M. M. Nor, Z. Ibarahim, N. H. A. Rasol, C. R. C. M. Zain, L. S. Joe, K. Ibrahim, N. Ahmad, N. M. Daud, ... S. C. Dzul-Kifli (Eds.), 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium (Vol. 1784). [040012] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966798
Shamsudin, Farha Mizana ; Radiman, Shahidan ; Abdullah, Yusof ; A. Hamid, Nasri. / Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy. 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. editor / Khairiah Hj. Basri ; Mohd Salmi Md Noorani ; Wan Zuhairi Wan Yaacob ; Mohd Firdaus Mohd Yusoff ; Nurul Huda Abd Karim ; Mohammad Hafizuddin Hj. Jumali ; Nazlina Ibrahim ; Muzzneena Ahmad Mustapha ; Zalita Zainuddin ; Nurulkamal Masseran ; Mahanem Mat Nor ; Zahari Ibarahim ; Noor Hayati Ahmad Rasol ; Che Radziah Che Mohd Zain ; Lim Seng Joe ; Kamarulzaman Ibrahim ; Norhayati Ahmad ; Norlida Mat Daud ; Syahida Che Dzul-Kifli. Vol. 1784 American Institute of Physics Inc., 2016.
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title = "Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy",
abstract = "Oxide dispersion strengthened (ODS) ferritic alloy containing 12wt{\%} Cr and 0.5wt{\%} Y2O3 was prepared by mechanical alloying (MA) method and then compacted into bulk shape. Field emission scanning electron microscopy (FESEM) was performed to characterize the microstructure of milled alloy powder. The fragments and nanoclusters of Y2O3 were observed in this alloy powder. FESEM-EDS mapping on the milled alloy powder reveal the uniformity of the element distribution achieved by the alloy. The Y element is finely dispersed into the alloy matrix and the O element is observed indicating the presence of oxides throughout the alloy sample. The compacted alloy was then heat treated at 1050°C and analyzed by field emission scanning electron microscope (FESEM). The formations of nano-scale Y2O3 were observed after the heat treatment process of alloy indicating the dispersion and incorporation of Y2O3 nanoparticles into the alloy matrix.",
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Shamsudin, FM, Radiman, S, Abdullah, Y & A. Hamid, N 2016, Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy. in KH Basri, MSM Noorani, WZW Yaacob, MFM Yusoff, NHA Karim, MHH Jumali, N Ibrahim, MA Mustapha, Z Zainuddin, N Masseran, MM Nor, Z Ibarahim, NHA Rasol, CRCM Zain, LS Joe, K Ibrahim, N Ahmad, NM Daud & SC Dzul-Kifli (eds), 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. vol. 1784, 040012, American Institute of Physics Inc., 2016 Postgraduate Colloquium of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology, UKM FST 2016, Selangor, Malaysia, 13/04/16. https://doi.org/10.1063/1.4966798

Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy. / Shamsudin, Farha Mizana; Radiman, Shahidan; Abdullah, Yusof; A. Hamid, Nasri.

2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. ed. / Khairiah Hj. Basri; Mohd Salmi Md Noorani; Wan Zuhairi Wan Yaacob; Mohd Firdaus Mohd Yusoff; Nurul Huda Abd Karim; Mohammad Hafizuddin Hj. Jumali; Nazlina Ibrahim; Muzzneena Ahmad Mustapha; Zalita Zainuddin; Nurulkamal Masseran; Mahanem Mat Nor; Zahari Ibarahim; Noor Hayati Ahmad Rasol; Che Radziah Che Mohd Zain; Lim Seng Joe; Kamarulzaman Ibrahim; Norhayati Ahmad; Norlida Mat Daud; Syahida Che Dzul-Kifli. Vol. 1784 American Institute of Physics Inc., 2016. 040012.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

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T1 - Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy

AU - Shamsudin, Farha Mizana

AU - Radiman, Shahidan

AU - Abdullah, Yusof

AU - A. Hamid, Nasri

PY - 2016/11/17

Y1 - 2016/11/17

N2 - Oxide dispersion strengthened (ODS) ferritic alloy containing 12wt% Cr and 0.5wt% Y2O3 was prepared by mechanical alloying (MA) method and then compacted into bulk shape. Field emission scanning electron microscopy (FESEM) was performed to characterize the microstructure of milled alloy powder. The fragments and nanoclusters of Y2O3 were observed in this alloy powder. FESEM-EDS mapping on the milled alloy powder reveal the uniformity of the element distribution achieved by the alloy. The Y element is finely dispersed into the alloy matrix and the O element is observed indicating the presence of oxides throughout the alloy sample. The compacted alloy was then heat treated at 1050°C and analyzed by field emission scanning electron microscope (FESEM). The formations of nano-scale Y2O3 were observed after the heat treatment process of alloy indicating the dispersion and incorporation of Y2O3 nanoparticles into the alloy matrix.

AB - Oxide dispersion strengthened (ODS) ferritic alloy containing 12wt% Cr and 0.5wt% Y2O3 was prepared by mechanical alloying (MA) method and then compacted into bulk shape. Field emission scanning electron microscopy (FESEM) was performed to characterize the microstructure of milled alloy powder. The fragments and nanoclusters of Y2O3 were observed in this alloy powder. FESEM-EDS mapping on the milled alloy powder reveal the uniformity of the element distribution achieved by the alloy. The Y element is finely dispersed into the alloy matrix and the O element is observed indicating the presence of oxides throughout the alloy sample. The compacted alloy was then heat treated at 1050°C and analyzed by field emission scanning electron microscope (FESEM). The formations of nano-scale Y2O3 were observed after the heat treatment process of alloy indicating the dispersion and incorporation of Y2O3 nanoparticles into the alloy matrix.

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M3 - Conference contribution

AN - SCOPUS:85014685684

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BT - 2016 UKM FST Postgraduate Colloquium

A2 - Basri, Khairiah Hj.

A2 - Noorani, Mohd Salmi Md

A2 - Yaacob, Wan Zuhairi Wan

A2 - Yusoff, Mohd Firdaus Mohd

A2 - Karim, Nurul Huda Abd

A2 - Jumali, Mohammad Hafizuddin Hj.

A2 - Ibrahim, Nazlina

A2 - Mustapha, Muzzneena Ahmad

A2 - Zainuddin, Zalita

A2 - Masseran, Nurulkamal

A2 - Nor, Mahanem Mat

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A2 - Joe, Lim Seng

A2 - Ibrahim, Kamarulzaman

A2 - Ahmad, Norhayati

A2 - Daud, Norlida Mat

A2 - Dzul-Kifli, Syahida Che

PB - American Institute of Physics Inc.

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Shamsudin FM, Radiman S, Abdullah Y, A. Hamid N. Microstructural characterization of oxide dispersion strengthened (ODS) Fe-12Cr-0.5Y2O3 alloy. In Basri KH, Noorani MSM, Yaacob WZW, Yusoff MFM, Karim NHA, Jumali MHH, Ibrahim N, Mustapha MA, Zainuddin Z, Masseran N, Nor MM, Ibarahim Z, Rasol NHA, Zain CRCM, Joe LS, Ibrahim K, Ahmad N, Daud NM, Dzul-Kifli SC, editors, 2016 UKM FST Postgraduate Colloquium: Proceedings of the Universiti Kebangsaan Malaysia, Faculty of Science and Technology 2016 Postgraduate Colloquium. Vol. 1784. American Institute of Physics Inc. 2016. 040012 https://doi.org/10.1063/1.4966798