Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method

Research output: Chapter in Book/Report/Conference proceedingConference contribution

1 Citation (Scopus)

Abstract

This study was conducted in order to investigate the effect of calcination time on phase and microstructural characteristics of intermetallic matric composite (IMC), NiAl-Al 2 O 3 powder. This powder was synthesized using gel combustion method with octyl alcohol as fuel. Upon completion of the combustion process, the loose powder was calcined at 1050°C for 1, 2 and 4 hours and characterized using XRD, FESEM and TEM. The crystallite size was calculated to be in the range of 29-30 nm. It was found that NiAl-Al 2 O 3 exhibits high crystalline structure after calcination for 4 hours. Furthermore, longer calcination time also cause growth of the particle size. Findings indicate that high crystalline nanostructured NiAl-Al 2 O 3 powder consisting of submicron particles can be successfully produced using gel combustion synthesis with longer calcination time.

Original languageEnglish
Title of host publicationProceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014
EditorsFauziah Othman, Aamir Hussain Bhat, Sujan Chowdhury, Norani Muti Binti Mohamed, Othman Bin Mamat, Patthi Bin Hussain
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735413160
DOIs
Publication statusPublished - 22 Jul 2015
Event23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014 - Tronoh, Malaysia
Duration: 10 Dec 201412 Dec 2014

Publication series

NameAIP Conference Proceedings
Volume1669
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014
CountryMalaysia
CityTronoh
Period10/12/1412/12/14

Fingerprint

combustion synthesis
combustion
roasting
powders
gel
gels
synthesis
transmission electron microscopy
alcohol
crystal structure
methodology
X-ray diffraction
particle size
intermetallics
alcohols
composite materials
effect
method
causes

All Science Journal Classification (ASJC) codes

  • Ecology, Evolution, Behavior and Systematics
  • Ecology
  • Plant Science
  • Physics and Astronomy(all)
  • Nature and Landscape Conservation

Cite this

Mohd Afandi, N., Abd. Manap, A. N., Yusof, S. N. A., Salim, M. A., Azim, M. A., Othman, S. Z., ... Misran, H. (2015). Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method In F. Othman, A. H. Bhat, S. Chowdhury, N. M. B. Mohamed, O. Bin Mamat, & P. Bin Hussain (Eds.), Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014 [4919180] (AIP Conference Proceedings; Vol. 1669). American Institute of Physics Inc.. https://doi.org/10.1063/1.4919180
Mohd Afandi, Nurfanizan ; Abd. Manap, Abreeza Noorlina ; Yusof, S. N.A. ; Salim, M. A. ; Azim, M. Al ; Othman, Siti Zubaidah ; Mohd Pauzi, Nur Irfah ; Omar, Nooririnah ; Misran, Halina. / Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014. editor / Fauziah Othman ; Aamir Hussain Bhat ; Sujan Chowdhury ; Norani Muti Binti Mohamed ; Othman Bin Mamat ; Patthi Bin Hussain. American Institute of Physics Inc., 2015. (AIP Conference Proceedings).
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title = "Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method",
abstract = "This study was conducted in order to investigate the effect of calcination time on phase and microstructural characteristics of intermetallic matric composite (IMC), NiAl-Al 2 O 3 powder. This powder was synthesized using gel combustion method with octyl alcohol as fuel. Upon completion of the combustion process, the loose powder was calcined at 1050°C for 1, 2 and 4 hours and characterized using XRD, FESEM and TEM. The crystallite size was calculated to be in the range of 29-30 nm. It was found that NiAl-Al 2 O 3 exhibits high crystalline structure after calcination for 4 hours. Furthermore, longer calcination time also cause growth of the particle size. Findings indicate that high crystalline nanostructured NiAl-Al 2 O 3 powder consisting of submicron particles can be successfully produced using gel combustion synthesis with longer calcination time.",
author = "{Mohd Afandi}, Nurfanizan and {Abd. Manap}, {Abreeza Noorlina} and Yusof, {S. N.A.} and Salim, {M. A.} and Azim, {M. Al} and Othman, {Siti Zubaidah} and {Mohd Pauzi}, {Nur Irfah} and Nooririnah Omar and Halina Misran",
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doi = "10.1063/1.4919180",
language = "English",
series = "AIP Conference Proceedings",
publisher = "American Institute of Physics Inc.",
editor = "Fauziah Othman and Bhat, {Aamir Hussain} and Sujan Chowdhury and Mohamed, {Norani Muti Binti} and {Bin Mamat}, Othman and {Bin Hussain}, Patthi",
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Mohd Afandi, N, Abd. Manap, AN, Yusof, SNA, Salim, MA, Azim, MA, Othman, SZ, Mohd Pauzi, NI, Omar, N & Misran, H 2015, Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method in F Othman, AH Bhat, S Chowdhury, NMB Mohamed, O Bin Mamat & P Bin Hussain (eds), Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014., 4919180, AIP Conference Proceedings, vol. 1669, American Institute of Physics Inc., 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014, Tronoh, Malaysia, 10/12/14. https://doi.org/10.1063/1.4919180

Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method . / Mohd Afandi, Nurfanizan; Abd. Manap, Abreeza Noorlina; Yusof, S. N.A.; Salim, M. A.; Azim, M. Al; Othman, Siti Zubaidah; Mohd Pauzi, Nur Irfah; Omar, Nooririnah; Misran, Halina.

Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014. ed. / Fauziah Othman; Aamir Hussain Bhat; Sujan Chowdhury; Norani Muti Binti Mohamed; Othman Bin Mamat; Patthi Bin Hussain. American Institute of Physics Inc., 2015. 4919180 (AIP Conference Proceedings; Vol. 1669).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

TY - GEN

T1 - Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method

AU - Mohd Afandi, Nurfanizan

AU - Abd. Manap, Abreeza Noorlina

AU - Yusof, S. N.A.

AU - Salim, M. A.

AU - Azim, M. Al

AU - Othman, Siti Zubaidah

AU - Mohd Pauzi, Nur Irfah

AU - Omar, Nooririnah

AU - Misran, Halina

PY - 2015/7/22

Y1 - 2015/7/22

N2 - This study was conducted in order to investigate the effect of calcination time on phase and microstructural characteristics of intermetallic matric composite (IMC), NiAl-Al 2 O 3 powder. This powder was synthesized using gel combustion method with octyl alcohol as fuel. Upon completion of the combustion process, the loose powder was calcined at 1050°C for 1, 2 and 4 hours and characterized using XRD, FESEM and TEM. The crystallite size was calculated to be in the range of 29-30 nm. It was found that NiAl-Al 2 O 3 exhibits high crystalline structure after calcination for 4 hours. Furthermore, longer calcination time also cause growth of the particle size. Findings indicate that high crystalline nanostructured NiAl-Al 2 O 3 powder consisting of submicron particles can be successfully produced using gel combustion synthesis with longer calcination time.

AB - This study was conducted in order to investigate the effect of calcination time on phase and microstructural characteristics of intermetallic matric composite (IMC), NiAl-Al 2 O 3 powder. This powder was synthesized using gel combustion method with octyl alcohol as fuel. Upon completion of the combustion process, the loose powder was calcined at 1050°C for 1, 2 and 4 hours and characterized using XRD, FESEM and TEM. The crystallite size was calculated to be in the range of 29-30 nm. It was found that NiAl-Al 2 O 3 exhibits high crystalline structure after calcination for 4 hours. Furthermore, longer calcination time also cause growth of the particle size. Findings indicate that high crystalline nanostructured NiAl-Al 2 O 3 powder consisting of submicron particles can be successfully produced using gel combustion synthesis with longer calcination time.

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U2 - 10.1063/1.4919180

DO - 10.1063/1.4919180

M3 - Conference contribution

AN - SCOPUS:85049329969

T3 - AIP Conference Proceedings

BT - Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014

A2 - Othman, Fauziah

A2 - Bhat, Aamir Hussain

A2 - Chowdhury, Sujan

A2 - Mohamed, Norani Muti Binti

A2 - Bin Mamat, Othman

A2 - Bin Hussain, Patthi

PB - American Institute of Physics Inc.

ER -

Mohd Afandi N, Abd. Manap AN, Yusof SNA, Salim MA, Azim MA, Othman SZ et al. Effect of calcination time on NiAl-Al 2 O 3 using gel combustion synthesis method In Othman F, Bhat AH, Chowdhury S, Mohamed NMB, Bin Mamat O, Bin Hussain P, editors, Proceedings of the 23rd Scientific Conference of Microscopy Society Malaysia, SCMSM 2014. American Institute of Physics Inc. 2015. 4919180. (AIP Conference Proceedings). https://doi.org/10.1063/1.4919180